Performance of SMB with conventional and monolith columns

• Tipo: Artigo em Revista Científica Internacional
• Data: 2008

Autores

Michal Zabka (Autor) FEUP; Pedro Sá Gomes (Autor) Outra; Alírio E. Rodrigues (Autor) FEUP

Revista

Título: Separation and Purification Technology

Vol. 63 Nº 2

Páginas: 324-333

ISSN: 1383-5866

Editora: Elsevier

Indexação

ISI Web of Knowledge - 9 Citações

ISI Web of Science

Scopus - 7 Citações

COMPENDEX

Classificação Científica

FOS: Ciências da engenharia e tecnologias

CORDIS: Ciências Tecnológicas > Engenharia > Engenharia química

Outras Informações

ID Authenticus: P-003-VFT

DOI: 10.1016/j.seppur.2008.05.018

Abstract (EN): In this article the performances of different bed structures, i.e., conventional adsorbent beads (with different diameters) and monolithic columns, in the separation of chiral species by the simulated moving bed (SMB) technology are compared. In order to assess these different morphologies the equivalent particle size for monolithic structure was calculated based on equivalent permeabilities. The performance of the SMB units was compared for the conditions quantified by maximum productivity. The configuration of the SMB unit and the total system volume were not varied. The maximum operating pressure drop of 20 bar and the purity in both product streams over 99% were set as constraints in all computations. The true moving bed model was used as an analogy to simulated moving bed in order to reduce computation time. The productivity of the SMB unit using particle diameter of 27 mu m can be slightly higher than of the SMB with particle diameter >= 50 mu m but at the cost of higher eluent consumption. Moreover, there is no need to operate an SMB unit at its maximum pressure drop to get the best performance values, since in the presence of mass-transfer resistances, the contact time becomes the unit major limitation. (C) 2008 Elsevier B.V. All rights reserved.

Idioma: Inglês

Tipo (Avaliação Docente): Científica