Separation Processes

Code:

EBE0130

Acronym:

PSEP

Keywords
Classification	Keyword
OFICIAL	Bioprocess Engineering
OFICIAL	Biological Engineering

Instance: 2012/2013 - 2S

Active?	Yes
Responsible unit:	Department of Chemical and Biological Engineering
Course/CS Responsible:	Master in Bioengineering

Cycles of Study/Courses

Acronym	No. of Students	Study Plan	Curricular Years	Credits UCN	Credits ECTS	Contact hours	Total Time
MIB	23	Syllabus	3	-	6	56	162

Teaching language

Portuguese

Objectives

The aim of this course unit is to illustrate the importance of separation and purification processes in the technical and economical feasibility of chemical, biological, and similar industrial processes, giving the students the necessary background for the selection, analysis and design of some of the most common separation processes that can be found in these industries.

Learning outcomes and competences

The students are expected to attain the following skills:

- Identification of the basic principles governing the different classes of separation processes;

- Selection of the process(es) more adequate to accomplish a desired separation/purification;

- Simplified design of the separation equipment studied, and understanding of the influence of the different operating conditions in the separation.

Working method

Presencial

Pre-requirements (prior knowledge) and co-requirements (common knowledge)

Knowledge of solution thermodynamics and mass end energy balances.

Program

INTRODUCTION: Characterization and classification of the separation processes. Notion of separating agent, recovery and purity. General criteria for the selection of separation processes.

SOLVENT EXTRACTION: The importance of solvent extraction. Liquid-Liquid and solid-liquid extraction processes. Description of the liquid-liquid and solid-liquid equilibrium. Extraction in a single equilibrium stage and in units with several equilibrium stages operating in cross and counter-current flow. Analysis of the influence of the different operating variables on the separation, using algebraic and graphic methods. Brief introduction to supercritical extraction, extraction in two aqueous phase systems, and the use of ionic liquids as solvents.

DISTILLATION: The importance of distillation in the chemical, biological and food industry. Design of flash units. Description of the vapour-liquid equilibrium. Binary distillation: application of the McCabe-Thiele method to conventional distillation columns and to columns with multiple feed streams and side products. Multicomponent distillation: the approximate method of Fenske – Underwood - Gilliland – Kirkbride. Definition of overall efficiency. Design of tray and pack columns.

GAS ABSORPTION: Solubility of gases in liquids. Design of absorption columns for dilute solutions: Kremser equation. Design of pack columns: definition of height and number of transfer units.

DRYING AND HUMIDIFICATION: Types of industrial dryers and their applications. Definition of absolute humidity, relative humidity, adiabatic saturation temperature, and wet bulb temperature. Use of the psychometric diagram. Drying velocity laws. Design of dryers. Brief introduction to the liofilization process.

EVAPORATION: Types of industrial evaporators and their applications. Economy and capacity of a system of evaporators. Calculation of the temperature of liquid solutions. Notion of boiling point rise (BPR). Analysis of a single effect evaporator. Design of multiple-effect evaporators operating in counter and co-current.

CRYSTALLIZATION: Types of crystallizers and their applications. Introduction to the theories of nucleation. Study of the growth of single crystals and their size distribution. Mass balance to crystallizers.

Mandatory literature

Domingos Barbosa; "Apontamentos de Processos de Separação", 2012
Edmundo Gomes de Azevedo e Ana Maria Alves; Engenharia de processos de separação. ISBN: 978-972-8469-80-1

Complementary Bibliography

Geankoplis, Christie J.; Transport processes and unit operations. ISBN: 0-13-045253-X
Warren L. McCabe, Julian C. Smith, Peter Harriott; Unit operations of Chemical Engineering. ISBN: 0-07-112738-0
J.D. Seader, Ernest J. Henley; Separation process principles. ISBN: 0-471-58626-9

Teaching methods and learning activities

Oral presentation of the theoretical concepts and analysis of problems exemplifying their application.

Evaluation Type

Distributed evaluation with final exam

Assessment Components

Description	Type	Time (hours)	Weight (%)	End date
Attendance (estimated)	Participação presencial	68,00
1st Test	Teste	2,00	33,30	2013-04-02
2nd Test	Teste	2,00	33,30	2013-05-14
3rd Test	Teste	2,00	33,40
	Total:	-	100,00

Eligibility for exams

According to FEUP's regulations.

Calculation formula of final grade

The student will take 3 tests during the semester.

The final classification will be the average grade of the three tests. The student can opt for taken a final exam.

Examinations or Special Assignments

Not applicable.

Internship work/project

Not applicable.

Special assessment (TE, DA, ...)

By exam.

Classification improvement

By exam.