Study of binary mixtures of Tribulus terrestris extract and Quillaja bark saponin as oil-in-water nanoemulsion emulsifiers

• Type: Article in International Scientific Journal
• Date: 2023

Authors

Schreiner, TB (Author) Other; Santamaria-Echart, A (Author) Other; Peres, AM (Author) Other; Madalena M. Dias (Author) FEUP; Pinho, SP (Author) Other; Barreiro, MF (Author) Other

Journal

Title: Journal of Surfactants and Detergents

ISSN: 1097-3958

Publisher: Wiley-Blackwell

Indexing

ISI Web of Knowledge - 0 Citations

Scopus - 0 Citations

Associated Projects

LA LSRE-LCM - Financiamento Plurianual 2020-2023 para a Unidade LA LSRE-LCM Laboratório de Processos de Separação e Reacção - Laboratório de Catálise e Materiais

Other information

Authenticus ID: P-00Z-2WC

DOI: 10.1002/jsde.12710

Abstract (EN): Several industrial fields use emulsifiers in their products, with the ones of natural origin gaining increasing relevance. Identifying and using diversified sources for their extraction is a pertinent topic regarding sustainability principles, biodiversity preservation, or cost rationalization. This is the case of Quillaja bark saponin (QS), for which saponin-rich extracts, for example, Tribulus terrestris (TT), are being highlighted as viable alternatives, even though constraints like performance are still on the table. In this context, an experimental design using binary emulsifier mixtures of TT with pure QS was carried out by changing their composition (50-90%wt. TT), content (1.5-4.5%wt.), and high-pressure homogenization conditions (5-15 cycles). The emulsions were characterized by zeta potential, morphology, droplet size, and stability (expressed as the number of days without creaming formation). Moreover, the cream index for 30 days was determined to indicate the destabilization extent. The zeta potential showed stable emulsions (values below -41 mV); even still, creaming formed for samples using a low emulsifier and high TT contents. The emulsions' mean droplet diameter (D [3, 2]) was between 78 and 921 nm, with smaller sizes agreeing with higher stability. The statistical analysis indicated an optimum composition range comprising an emulsifier content between 3.9 and 4.5%wt. and TT content between 50 and 56%wt. to reach stable products. Overall, TT can provide an effective solution when combined with QS, decreasing the dependence on Quillaja bark.

Language: English

Type (Professor's evaluation): Scientific

No. of pages: 11