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Palladium-catalysed reactions of 8-hydroxy- and 8-benzyloxy-5,7-diiodoquinoline under aminocarbonylation conditions

Title
Palladium-catalysed reactions of 8-hydroxy- and 8-benzyloxy-5,7-diiodoquinoline under aminocarbonylation conditions
Type
Article in International Scientific Journal
Year
2011
Authors
Takacs, A
(Author)
Other
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Szilagyi, A
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Acs, P
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Mark, L
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Peixoto, AF
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Pereira, MM
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Kollar, L
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Journal
Title: TetrahedronImported from Authenticus Search for Journal Publications
Vol. 67
Pages: 2402-2406
ISSN: 0040-4020
Publisher: Elsevier
Other information
Authenticus ID: P-002-SZ5
Abstract (EN): Various 5-carboxamido-7-iodo-8-benzyloxyquinolines were synthesised via selective aminocarbonylation of 5,7-diiodo-8-benzyloxyquinoline in the presence of in situ generated palladium(0) catalysts. Under similar conditions (50 degrees C. 80 bar CO), 5,7-bis(N-tert-butyl-glyoxylamido)-8-hydroxyquinoline was obtained using tert-butylamine as N-nucleophile. The unprotected 5,7-diiodo-8-hydroxyquinoline underwent dehydroiodination resulting in 8-hydroxyquinoline as the major product.
Language: English
Type (Professor's evaluation): Scientific
No. of pages: 5
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