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Response surface optimisation applied to a headspace-solid phase microextraction-gas chromatography-mass spectrometry method for the analysis of volatile organic compounds in water matrices

Title
Response surface optimisation applied to a headspace-solid phase microextraction-gas chromatography-mass spectrometry method for the analysis of volatile organic compounds in water matrices
Type
Article in International Scientific Journal
Year
2012
Authors
Vera Homem
(Author)
FEUP
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Raquel Sousa
(Author)
FEUP
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José Luís Moreira
(Author)
FEUP
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Lúcia Santos
(Author)
FEUP
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Arminda Alves
(Author)
FEUP
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Journal
Vol. 92 No. 2
Pages: 166-189
ISSN: 0306-7319
Publisher: Taylor & Francis
Indexing
Publicação em ISI Web of Science ISI Web of Science
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Scientific classification
FOS: Natural sciences > Chemical sciences
Other information
Authenticus ID: P-002-HDJ
Abstract (EN): A new method for the simultaneous determination of 12 volatile organic compounds (trans-1,2-dichloroethene, 1,1,1-trichloroethane, benzene, 1,2-dichloroethane, trichloroethene, toluene, 1,1,2-trichloroethane, tetrachloroethene, ethylbenzene, m-, p-, o-xylene) in water samples by headspace solid phase microextraction (HS-SPME)-gas chromatography mass spectrometry (GC-MS) was described, using a 100 mm PDMS (polydimethylsiloxane) coated fibre. The response surface methodology was used to optimise the effect of the extraction time and temperature, as well as the influence of the salt addition in the extraction process. Optimal conditions were extraction time and temperature of 30 min and -20 degrees C, respectively, and NaCl concentration of 4 mol L(-1). The detection limits were in the range of 1.1 x 10(-3)-2.3 mu g L(-1) for the 12 volatile organic compounds (VOCs). Global uncertainties were in the range of 4-68%, when concentrations decrease from 250 mu g L(-1) down to the limits of quantification. The method proved adequate to detect VOCs in six river samples.
Language: English
Type (Professor's evaluation): Scientific
No. of pages: 24
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