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Agar extraction from integrated multitrophic aquacultured Gracilaria vermiculophylla: Evaluation of a microwave-assisted process using response surface methodology

Title
Agar extraction from integrated multitrophic aquacultured Gracilaria vermiculophylla: Evaluation of a microwave-assisted process using response surface methodology
Type
Article in International Scientific Journal
Year
2010
Authors
A.M.M. Sousa
(Author)
FEUP
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V. D. Alves
(Author)
FEUP
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S. Morais
(Author)
FEUP
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C. Delerue-Matos
(Author)
FEUP
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M. P. Gonçalves
(Author)
FEUP
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Journal
Vol. 101
Pages: 3258-3267
ISSN: 0960-8524
Publisher: Elsevier
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Publicação em ISI Web of Science ISI Web of Science
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Scientific classification
FOS: Engineering and technology > Other engineering and technologies
Other information
Authenticus ID: P-003-6W4
Abstract (EN): Microwave-assisted extraction (MAE) of agar from Gracilaria vermiculophylla, produced in an integrated multitrophic aquaculture (IMTA) system, from Ria de Aveiro (northwestern Portugal), was tested and optimized using response surface methodology. The influence of the MAE operational parameters (extraction time, temperature, solvent volume and stirring speed) on the physical and chemical properties of agar (yield, gel strength, gelling and melting temperatures, as well as, sulphate and 3,6-anhydro-L-galactose contents) was evaluated in a 2(4) orthogonal composite design. The quality of the extracted agar compared favorably with the attained using traditional extraction (2 h at 85 degrees C) while reducing drastically extraction time, solvent consumption and waste disposal requirements. Agar MAE optimum results were: an yield of 14.4 +/- 0.4%, a gel strength of 1331 +/- 51 g/cm(2), 40.7 +/- 0.2 degrees C gelling temperature, 93.1 +/- 0.5 degrees C melting temperature, 1.73 +/- 0.13% sulfate content and 39.4 +/- 0.3% 3,6-anhydro-L-galactose content. Furthermore, this study suggests the feasibility of the exploitation of G. vermiculophylla grew in IMTA systems for agar production.
Language: English
Type (Professor's evaluation): Scientific
No. of pages: 10
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