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Pyroelectric current spectroscopy: example of application on Nb doped Pb(Zr0.92Ti0.08)O-3 ceramics for infrared detection

Title
Pyroelectric current spectroscopy: example of application on Nb doped Pb(Zr0.92Ti0.08)O-3 ceramics for infrared detection
Type
Article in International Scientific Journal
Year
2004
Authors
Pintilie, L
(Author)
Other
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Pereira, M
(Author)
Other
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Gomes, MJM
(Author)
Other
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Boerasu, I
(Author)
Other
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Journal
Vol. 115
Pages: 185-190
ISSN: 0924-4247
Publisher: Elsevier
Other information
Authenticus ID: P-000-8GM
Abstract (EN): Pyroelectric current spectroscopy (PCS) was used to investigate the homogeneity of the Nb doped lead zirconate-titanate Pb(Zr-0.92 Ti-0.08)O-3, (PZT) ceramics intended to be used in the infrared (IR) pyroelectric detectors manufacturing. The non-homogeneous composition in the ceramic volume is reflected by the occurrence of several peaks in the PCS spectra, suggesting the presence of PZT phases with different Zr/Ti ratio, thus having different transition temperatures. The non-homogeneity was confirmed by compositional analysis performed using an Energy Dispersive X-ray Spectrometer (EDAX) attached to a Scanning Electron Microscope (SEM). PCS can be a useful tool in optimizing the calcination and sintering parameters (temperature and time) during ceramic preparation.
Language: English
Type (Professor's evaluation): Scientific
No. of pages: 6
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