Automatized and desktop AC-susceptometer for the in situ and real time monitoring of magnetic nanoparticles' synthesis by coprecipitation

• Type: Article in International Scientific Journal
• Date: 2015

Authors

Fernandez Garcia, MP (Author) Other; Teixeira, JM (Author) Other; Machado, P (Author) Other; Oliveira, MRFF (Author) Other; Maia, JM (Author) Other; Clara Pereira (Author) FCUP; pereira, a. m. (Author) FCUP; Cristina Freire (Author) FCUP; araujo, j. p. (Author) FCUP

Journal

Title: Review of Scientific Instruments

Vol. 86

Final page: 043904

ISSN: 0034-6748

Publisher: American Institute of Physics

Indexing

ISI Web of Knowledge - 7 Citations

Scopus - 6 Citations

Other information

Authenticus ID: P-00A-D09

DOI: 10.1063/1.4918723

Abstract (EN): The main purpose of this work was to design, develop, and construct a simple desktop AC susceptometer to monitor in situ and in real time the coprecipitation synthesis of magnetic nanoparticles. The design incorporates one pair of identical pick-up sensing coils and one pair of Helmholtz coils. The picked up signal is detected by a lock-in SR850 amplifier that measures the in-and out-of-phase signals. The apparatus also includes a stirrer with 45 degrees-angle blades to promote the fast homogenization of the reaction mixture. Our susceptometer has been successfully used to monitor the coprecipitation reaction for the synthesis of iron oxide nanoparticles. (C) 2015 AIP Publishing LLC.

Language: English

Type (Professor's evaluation): Scientific

No. of pages: 6