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Formulation, rheology and thermal ageing of polymer greases-Part I: Influence of the thickener content

Title
Formulation, rheology and thermal ageing of polymer greases-Part I: Influence of the thickener content
Type
Article in International Scientific Journal
Year
2015
Authors
Graca, B
(Author)
Other
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Campos, AV
(Author)
Other
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Jorge Seabra
(Author)
FEUP
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Leckner, J
(Author)
Other
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Westbroek, R
(Author)
Other
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Journal
Vol. 87
Pages: 160-170
ISSN: 0301-679X
Publisher: Elsevier
Other information
Authenticus ID: P-00G-42V
Abstract (EN): The aim of this work is to show the correlation between polymer greases' rheology and its formulation. The tested polypropylene (PP) thickened greases were evaluated regarding their thickener content and its effect on the rheological properties. An artificial ageing procedure was performed by heating fresh grease samples in an oven to study the thermal degradation. The ageing evaluation was performed through rheological measurements, FT-IR spectra, oil loss, bleed-oil viscosity changes and bleed rate. The rheology measurements were performed on a rotational rheometer, emphasizing on the storage and loss moduli values at the Linear Visco-Elastic (LVE) region. The flow curve of each grease was also measured. A modified Herschel-Buckley model was applied and the data was correlated to the thickener content.
Language: English
Type (Professor's evaluation): Scientific
No. of pages: 11
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